|
PREPARING
YOUR SAMPLE |
|
|
|
|
|
|
Help!
I don't know anything about my sample! |
|
You may
know more than you think. Where did the sample come from? If you prepared
it yourself, you should have some idea of the chemistry involved. Even
if you are not sure of the exact structure, can you at least put it into
a general class of compound? Ask yourself: |
|
|
|
Is
it aliphatic, olefinic, or aromatic? |
|
|
|
Is
it halogenated? |
|
|
|
Is
it likely to contain any elements other than carbon, hydrogen, or a halogen?
Such elements might include oxygen, nitrogen, sulfur, phosphorus. or silicon? |
|
|
|
Is
it likely to have any functional groups, such as hydroxyls, carbonyls,
or amines? |
|
|
|
Do
you have enough to record an infrared spectrum? Even if a definitive identification
can't be made, this may provide some clues that enable you to answer some
of the questions above. |
|
|
|
Do
you have enough material to do some solubility tests? Check a variety
of solvents to see which ones dissolve your sample. For example, you might
try chloroform, benzene, acetone, methanol, and water. |
|
|
|
|